1-fluoro-2,5-dimethoxy-4-nitrobenzene

Martin Sweeney; Patrick McArdle; Fawaz Aldabbagh

doi:10.13025/28680

1-fluoro-2,5-dimethoxy-4-nitrobenzene

Martin Sweeney
, Patrick McArdle
, Fawaz Aldabbagh

University of Galway
Kingston University

Research output: Contribution to a Journal (Peer & Non Peer) › Article › peer-review

Abstract

1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by ¹H and¹³C-NMR, elemental analysis, EI-MS and FT-IR.

Original language	English
Article number	M984
Journal	MolBank
Volume	2018
Issue number	1
DOIs	https://doi.org/10.13025/28680 https://doi.org/10.3390/m984
Publication status	Published - Mar 2018
Externally published	Yes

Keywords

Fluorobenzene
Nitration
Nucleophilic aromatic substitution
X-ray crystallography

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10.13025/28680Licence: CC BY-NC-ND
10.3390/m984

Cite this

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title = "1-fluoro-2,5-dimethoxy-4-nitrobenzene",

abstract = "1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90\% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by 1H and13C-NMR, elemental analysis, EI-MS and FT-IR.",

keywords = "Fluorobenzene, Nitration, Nucleophilic aromatic substitution, X-ray crystallography",

author = "Martin Sweeney and Patrick McArdle and Fawaz Aldabbagh",

note = "Publisher Copyright: {\textcopyright} 2018 by the authors. Licensee MDPI, Basel, Switzerland.",

year = "2018",

month = mar,

doi = "10.13025/28680",

language = "English",

volume = "2018",

journal = "MolBank",

issn = "1422-8599",

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T1 - 1-fluoro-2,5-dimethoxy-4-nitrobenzene

AU - Sweeney, Martin

AU - McArdle, Patrick

AU - Aldabbagh, Fawaz

PY - 2018/3

Y1 - 2018/3

N2 - 1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by 1H and13C-NMR, elemental analysis, EI-MS and FT-IR.

AB - 1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by 1H and13C-NMR, elemental analysis, EI-MS and FT-IR.

KW - Fluorobenzene

KW - Nitration

KW - Nucleophilic aromatic substitution

KW - X-ray crystallography

UR - http://hdl.handle.net/10379/14089

UR - https://www.scopus.com/pages/publications/85042522593

U2 - 10.13025/28680

DO - 10.13025/28680

M3 - Article

SN - 1422-8599

VL - 2018

JO - MolBank

JF - MolBank

IS - 1

M1 - M984

ER -

1-fluoro-2,5-dimethoxy-4-nitrobenzene

Abstract

Keywords

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